一种废旧涤纶纺织品完全醇解纺制再生纤维的工艺

文档序号:184424 发布日期:2021-11-02 浏览:56次 >En<

阅读说明:本技术 一种废旧涤纶纺织品完全醇解纺制再生纤维的工艺 (Process for spinning regenerated fibers by complete alcoholysis of waste polyester textiles ) 是由 肖洪卫 成强 张昕 于 2021-07-15 设计创作,主要内容包括:本发明涉及一种废旧涤纶纺织品完全醇解纺制再生纤维的工艺,包括以下步骤:1挑选、分拣;2撕碎;3混料;4物料缓存;5密实处理;6预醇解;7粗过滤;8一次精过滤;9深度醇解;10二次精过滤;11低沸物脱除;12高沸物脱除;13预缩聚;14终缩聚;15熔体精过滤;16纺丝;17冷却成形;18上油卷绕;19多道牵伸;20卷曲;21定型;22切断;23打包。本发明通过废旧涤纶纺织品完全醇解,醇解液过滤除去低聚物、机械杂质;过滤得到的醇解液进行两次纯化脱杂,脱除低沸物、高沸物得到高纯度对苯二甲酸二乙二醇酯(BHET);高纯度对苯二甲酸二乙二醇酯(BHET)聚合后得到粘度高、分子量分布窄、端羧基含量低、可纺性好、品质均一的再生纤维。(The invention relates to a process for spinning regenerated fibers by complete alcoholysis of waste polyester textiles, which comprises the following steps: 1, selecting and sorting; 2, shredding; 3, mixing materials; 4, caching materials; 5, compacting; 6, pre-alcoholysis; 7, coarse filtration; 8, fine filtering for one time; 9 deep alcoholysis; 10, fine filtering for twice; 11, removing low-boiling-point substances; removing 12 high-boiling-point substances; 13 pre-polycondensation; 14 final polycondensation; 15 fine filtering the melt; 16 spinning; 17 cooling and forming; 18, oiling and winding; 19, multi-pass drawing; 20, curling; 21, shaping; 22, cutting off; and 23, packaging. The method comprises the steps of completely alcoholyzing the waste polyester textiles, and filtering alcoholysis liquid to remove oligomers and mechanical impurities; purifying and removing impurities twice from the alcoholysis solution obtained by filtering, and removing low-boiling-point substances and high-boiling-point substances to obtain high-purity diethylene glycol terephthalate (BHET); the high-purity diethylene glycol terephthalate (BHET) is polymerized to obtain the regenerated fiber with high viscosity, narrow molecular weight distribution, low carboxyl end group content, good spinnability and uniform quality.)

一种废旧涤纶纺织品完全醇解纺制再生纤维的工艺

技术领域

本发明涉及一种废旧涤纶纺织品完全醇解纺制再生纤维的工艺,属于废旧涤纶纺织品的再生领域。

背景技术

随着涤纶纺织品的使用量增加,人们也逐渐重视废旧涤纶纺织品的再生领域研究。目前,废旧涤纶纺织品纺制再生纤维的常用工艺是废旧涤纶纺织品螺杆熔融、纺丝和废旧涤纶纺织品螺杆熔融、均化增粘、纺丝。不论哪种工艺,均依赖于废旧涤纶纺织品的品质,容易造成每批产品粘度不稳定、重复性差、可纺性不稳定,对于品质差的废旧涤纶纺织品,甚至无法纺丝。

10页详细技术资料下载
上一篇:一种医用注射器针头装配设备
下一篇:一种羊绒条干的加工设备

网友询问留言

已有0条留言

还没有人留言评论。精彩留言会获得点赞!

精彩留言,会给你点赞!